Spectroscopy, chromatography and microscopic image of 3-(4-methoxyphenyl)-1-phenylprop-2-en-1-one (MNYAD_1539) crystals

Munshi, Tasnim, Abdull Manap, Mohd Rashidi, Scowen, Ian , Risdan, Muhammad Najmi, Shamsul Ariffin, Muhammad Danial Ariffin, Alkaf, Atiqah Dalia, Abdul Aziz, Nurhayani and Ismail, Mohd Farid (2019) Spectroscopy, chromatography and microscopic image of 3-(4-methoxyphenyl)-1-phenylprop-2-en-1-one (MNYAD_1539) crystals. In: Industrial Chemistry Seminar (SKI), 15th January 2019, Bangi Resort Hotel, Malaysia.

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Spectroscopy, chromatography and microscopic image of 3-(4-methoxyphenyl)-1-phenylprop-2-en-1-one (MNYAD_1539) crystals
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Item Type:Conference or Workshop contribution (Poster)
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Abstract

3-(4-methoxyphenyl)-1-phenylprop-2-en-1-one (MNYAD_1539) was synthesized by an Aldol condensation method . MNYAD_1539 was synthesized from two commercially available materials of p-Methoxybenzaldehyde and Acetophenone The physical and chemical properties of MNYAD_1539 was investigated using ATR-FTIR, GCMS and a microscope. The FTIR spectrum of the crude MNYAD_1539 showed the presence of impurities, compared with the crystalline sample. The chromatogram showed that MNYAD_1539 with high purity was produced after re-crystallisation. The current study also found high quality of the transparent needle-like crystal after re-crystallisation.

Keywords:Vibrational spectroscopy, gas chromatography-mass spectrometry
Subjects:F Physical Sciences > F100 Chemistry
Divisions:College of Science > School of Chemistry
ID Code:35973
Deposited On:16 May 2019 10:00

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